N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

Base Information

Chemical Name:N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide
CAS No.:850148-20-8
Molecular Formula:C₂₅H₂₄ClN₅O₄S
Molecular Weight:526.016
Hs Code.:

Synonyms:N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

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Chemical Property of N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

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Technology Process of N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

There total 2 articles about N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 850148-18-4
(2-amino-5-acetic acid methyl ester sulfanyl-phenyl)-N-(5-chloro-(2-pyridyl))carboxamide

: 850148-20-8
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0.5 h / 20 °C

2.1: hydrogen sulfide; triethylamine / pyridine / 3.17 h / 20 °C

2.2: 1.5 h / Heating / reflux

3.1: acetic acid / tetrahydrofuran; methanol / 0.67 h / Heating / reflux

With hydrogen sulfide; acetic acid; triethylamine; In tetrahydrofuran; pyridine; methanol;

Reference yield:

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 850148-20-8
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate / pyridine / 0.5 h

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 50 °C

3.1: tin(ll) chloride / ethyl acetate / 0.5 h / Heating / reflux

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: hydrogen sulfide; triethylamine / pyridine / 3.17 h / 20 °C

5.2: 1.5 h / Heating / reflux

6.1: acetic acid / tetrahydrofuran; methanol / 0.67 h / Heating / reflux

With hydrogen sulfide; caesium carbonate; acetic acid; triethylamine; tin(ll) chloride; trichlorophosphate; In tetrahydrofuran; pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide;