N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

Base Information

Chemical Name:N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide
CAS No.:850148-21-9
Molecular Formula:C₂₄H₂₂ClN₅O₄S
Molecular Weight:511.989
Hs Code.:

Synonyms:N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

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Chemical Property of N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

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Technology Process of N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

There total 3 articles about N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 850148-20-8
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

: 850148-21-9
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

Guidance literature:: With lithium hydroxide; water; In methanol; at 20 ℃; for 0.5h;

Reference yield:

: 850148-18-4
(2-amino-5-acetic acid methyl ester sulfanyl-phenyl)-N-(5-chloro-(2-pyridyl))carboxamide

: 850148-21-9
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 0.5 h / 20 °C

2.1: hydrogen sulfide; triethylamine / pyridine / 3.17 h / 20 °C

2.2: 1.5 h / Heating / reflux

3.1: acetic acid / tetrahydrofuran; methanol / 0.67 h / Heating / reflux

4.1: lithium hydroxide; water / methanol / 0.5 h / 20 °C

With lithium hydroxide; hydrogen sulfide; water; acetic acid; triethylamine; In tetrahydrofuran; pyridine; methanol;

Reference yield:

: N-(5-chloro(2-pyridyl)){5-acetic acid methyl ester sulfanyl-2-[(4-(iminomethylthiomethyl)phenyl)carbonylamino]phenyl}carboxamide

: 850148-21-9
N-(5-chloro-2-pyridinyl)-2-(4-N,N-dimethylamidinophenylcarbonyl)amino-5-acetic acid sulfanyl-phenylcarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / tetrahydrofuran; methanol / 0.67 h / Heating / reflux

2: lithium hydroxide; water / methanol / 0.5 h / 20 °C

With lithium hydroxide; water; acetic acid; In tetrahydrofuran; methanol;