methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

Base Information

Chemical Name:methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate
CAS No.:126623-88-9
Molecular Formula:C₁₄H₁₃ClN₂O₇S
Molecular Weight:388.785
Hs Code.:

Synonyms:methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

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Chemical Property of methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

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Technology Process of methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

There total 1 articles about methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67-56-1
methanol

: 126623-86-7
ethyl 3-(p-chlorophenyl)-4-<<(ethoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

: 126623-88-9
methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

Guidance literature:: With sulfuric acid; for 96h; Heating;
DOI:10.1002/hlca.19890720630

Reference yield: 54.0%

: 126623-88-9
methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

: 126623-92-5
methyl 3-(p-chlorophenyl)-7-hydroxy-5H-isoxazolo<5,4-e><1,2>thiazine-6-carboxylate 4,4-dioxide

Guidance literature:: With sodium methylate; In pyridine; at 20 ℃; for 22h;
DOI:10.1002/hlca.19890720630

Reference yield:

: 126623-88-9
methyl 3-(p-chlorophenyl)-4<<(methoxycarbonyl)methyl>sulfamoyl>isoxazole-5-carboxylate

: methyl 3-(p-chlorophenyl)-7-hydroxy-5-methyl-5H-isoxazolo<5,4-e><1,2>thiazine-6-carboxylate 4,4-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / NaOMe / pyridine / 22 h / 20 °C

2: 69 percent / NaH / dimethylformamide / 1.) 20 deg C, 1 h; 2.) 10 min

With sodium methylate; sodium hydride; In pyridine; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720630