C₂₇H₂₃N₅O₄

Base Information

Chemical Name:C₂₇H₂₃N₅O₄
CAS No.:135761-87-4
Molecular Formula:C₂₇H₂₃N₅O₄
Molecular Weight:481.511
Hs Code.:

C<sub>27</sub>H<sub>23</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₇H₂₃N₅O₄

Suppliers and Price of C₂₇H₂₃N₅O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of C₂₇H₂₃N₅O₄

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₂₃N₅O₄

There total 13 articles about C₂₇H₂₃N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1074-82-4
potassium phtalimide

: 135761-86-3
4-(2-azidophenyl)-6-<2-<(methylsulfonyl)oxy>ethyl>-5,6,7,8-tetrahydroquinolin-8-one ethylene ketal

: 135761-87-4
C₂₇H₂₃N₅O₄

Guidance literature:: In N,N-dimethyl-formamide; at 50 ℃; for 18h;
DOI:10.1021/ja00021a031

Reference yield:

: 51656-91-8
ethyl 1,4-dioxaspiro[4,5]dec-8-ylideneacetate

: 135761-87-4
C₂₇H₂₃N₅O₄

Guidance literature:: Multi-step reaction with 12 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 0.33 h / 108601 Torr / Ambient temperature

2: 90 percent / LAH / diethyl ether / -20 °C

3: 99 percent / aq. HCl / tetrahydrofuran

4: 88 percent / aq. NaOH / ethanol / 0.5 h / Ambient temperature

5: 99 percent / pyridine / Ambient temperature

6: Yb(fod)3 / 1,2-dichloro-ethane / 24 h / Heating

7: 56 percent / hydroxylamine hydrochloride / acetonitrile / Heating

8: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C, 2.) MeOH, from -78 deg C to RT, 1.5 h

9: 90 percent / HC(OEt)3, camphorsulfonic acid / 72 h / 60 °C

10: 99 percent / K₂CO₃ / methanol / 1.5 h / Ambient temperature

11: 100 percent / Et₃N / CH₂Cl₂ / 0 °C

12: 90 percent / dimethylformamide / 18 h / 50 °C

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium; dimethylsulfide; camphor-10-sulfonic acid; hydroxylamine hydrochloride; hydrogen; potassium carbonate; ozone; triethylamine; orthoformic acid triethyl ester; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00021a031

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 135761-87-4
C₂₇H₂₃N₅O₄

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) t-BuOK / 1.) DME, from 0 deg C to RT, 2.) DME, RT

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 0.33 h / 108601 Torr / Ambient temperature

3: 90 percent / LAH / diethyl ether / -20 °C

4: 99 percent / aq. HCl / tetrahydrofuran

5: 88 percent / aq. NaOH / ethanol / 0.5 h / Ambient temperature

6: 99 percent / pyridine / Ambient temperature

7: Yb(fod)3 / 1,2-dichloro-ethane / 24 h / Heating

8: 56 percent / hydroxylamine hydrochloride / acetonitrile / Heating

9: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C, 2.) MeOH, from -78 deg C to RT, 1.5 h

10: 90 percent / HC(OEt)3, camphorsulfonic acid / 72 h / 60 °C

11: 99 percent / K₂CO₃ / methanol / 1.5 h / Ambient temperature

12: 100 percent / Et₃N / CH₂Cl₂ / 0 °C

13: 90 percent / dimethylformamide / 18 h / 50 °C

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium; dimethylsulfide; camphor-10-sulfonic acid; hydroxylamine hydrochloride; potassium tert-butylate; hydrogen; potassium carbonate; ozone; triethylamine; orthoformic acid triethyl ester; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00021a031