1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

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Chemical Name:1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide
CAS No.:418772-22-2
Molecular Formula:Br*C₂₁H₂₃BrN
Molecular Weight:449.228
Hs Code.:

Synonyms:1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

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Chemical Property of 1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

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Technology Process of 1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

There total 5 articles about 1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4133-35-1
6-bromo-2-tetralone

: 100-39-0
benzyl bromide

: 418772-22-2
1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

Guidance literature:: 6-bromo-2-tetralone; With pyrrolidine; In toluene; at 150 ℃; for 2h; Heating / reflux;

benzyl bromide; In toluene; at 90 ℃; for 2.5h; Heating / reflux;

Reference yield: 73.0%

: 123-75-1
pyrrolidine

: 4133-35-1
C₁₀H₁₀BrO₄S^(1-)*Na⁽¹⁺⁾

: 100-39-0
benzyl bromide

: 418772-22-2
1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

Guidance literature:: C₁₀H₁₀BrO₄S^(1-)*Na⁽¹⁺⁾; With sodium hydrogencarbonate; In water; ethyl acetate;

pyrrolidine; In toluene; at 150 ℃; for 2h;

benzyl bromide; at 90 ℃; for 2h;

Reference yield: 73.0%

: 123-75-1
pyrrolidine

: bisulfite adduct of 6-bromo-2-tetralone

: 100-39-0
benzyl bromide

: 418772-22-2
1-(1-(RS)-benzyl-6-bromo-3,4-dihydro-1H-naphthalen-2-ylidene)-pyrrolidinium bromide

Guidance literature:: bisulfite adduct of 6-bromo-2-tetralone; With sodium hydrogencarbonate; In ethyl acetate;

pyrrolidine; In ethyl acetate; toluene; at 20 - 150 ℃;

benzyl bromide; In ethyl acetate; toluene; at 20 - 90 ℃;