5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one

Base Information

• Chemical Name: 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one
• CAS No.: 222965-37-9
• Molecular Formula: C₁₉H₁₈O₄
• Molecular Weight: 310.35
• Mol file: 222965-37-9.mol

Synonyms:5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one

Chemical Property of 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one

There total 1 articles about 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5,6-dimethoxy-1-indanone (2107-69-9) + 4-methoxy-benzaldehyde (123-11-5) → 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one (222965-37-9)

Guidance literature:

5,6-dimethoxy-1-indanone; With potassium hydroxide; In methanol; at 0 ℃;

4-methoxy-benzaldehyde; In methanol; at 0 - 40 ℃;

With hydrogenchloride;

DOI:10.1039/c4ra03823a

Reference yield: 80.0%

L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + 5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one (222965-37-9) + indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1) → 5'-benzyl-5,6-dimethoxy-2,3-dihydro-4'-(4-methoxyphenyl)dispiro[1H-indene-2,3'-pyrrolidine-2',3''-indoline]-1,2''-dione

Guidance literature:

at 100 ℃; for 1h; stereoselective reaction; Ionic liquid; Green chemistry;

DOI:10.3390/molecules20022296

Reference yield: 79.0%

5,6-dimethoxy-2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one (222965-37-9) + L-Tryptophan (73-22-3,27732-43-0,80206-30-0,27813-82-7) + acenaphthene quinone (82-86-0) → C41H34N2O5

Guidance literature:

With 1-n-butyl-3-methylimidazolim bromide; at 100 ℃; for 1h; diastereoselective reaction; Green chemistry;

DOI:10.1071/CH14370

upstream raw materials:

5,6-dimethoxy-1-indanone

4-methoxy-benzaldehyde

Downstream raw materials:

C₂₆H₂₄N₄O₆

C₂₆H₂₄ClN₃O₄

C₂₆H₂₄FN₃O₄

3-(4-methoxyphenyl)-N-(4-bromophenyl)-6,7-dimethoxy-3a,4-dihydro-3H-indeno[1,2-c]pyrazole-2-carboxamide