[2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

Base Information

Chemical Name:[2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester
CAS No.:1276121-44-8
Molecular Formula:C₂₁H₃₂N₂O₆
Molecular Weight:408.495
Hs Code.:

Synonyms:[2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

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Chemical Property of [2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

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Technology Process of [2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

There total 2 articles about [2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 19023-94-0
(2-aminoethyl)-methylcarbamic acid,benzyl ester

: 1276121-44-8
[2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

Guidance literature:: With dmap; triethylamine; In 1,2-dichloro-ethane; at 20 - 60 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1221593-52-7
methyl-[2-(2,2,2-trifluoro-acetylamino)-ethyl]carbamic acid benzyl ester

: 1276121-44-8
[2-(benzyloxycarbonyl-methyl-amino)-ethyl]-dicarbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / water; methanol / 3 h / 20 °C

2: triethylamine; dmap / 1,2-dichloro-ethane / 18 h / 20 - 60 °C / Inert atmosphere

With dmap; triethylamine; lithium hydroxide; In methanol; water; 1,2-dichloro-ethane;