7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

Base Information

Chemical Name:7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)
CAS No.:1370018-87-3
Molecular Formula:C₃₄H₂₆N₄O₄
Molecular Weight:554.605
Hs Code.:

Synonyms:7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

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Technology Process of 7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

There total 3 articles about 7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₈N₄O₆

: 98-86-2
acetophenone

: 1370018-87-3
7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

Guidance literature:: With piperidine; In ethanol; at 80 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.02.004

Reference yield:

: 86453-94-3,74917-84-3
3-methyl-4-nitro-5-(2-methylstyryl)isoxazole

: 1370018-87-3
7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 1 h / 80 °C

2: piperidine / ethanol / 3 h / 80 °C

With piperidine; In ethanol; 1: Michael condensation;
DOI:10.1016/j.ejmech.2012.02.004

Reference yield:

: 1123-49-5
3,5-dimethyl-4-nitroisoxazole

: 1370018-87-3
7,7'-(2-methylphenylmethylene)bis(3-methyl-6-phenylisoxazolo[4,5-b]pyridine-N-oxide)

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / ethanol / 0.5 h / Reflux

2: piperidine / ethanol / 1 h / 80 °C

3: piperidine / ethanol / 3 h / 80 °C

With piperidine; In ethanol; 1: Knoevenagel condensation / 2: Michael condensation;
DOI:10.1016/j.ejmech.2012.02.004