trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium

Base Information

Chemical Name:trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium
CAS No.:189276-42-4
Molecular Formula:C₄₅H₄₂As₂FIOPdSi
Molecular Weight:1029.08
Hs Code.:

Synonyms:trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium

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Chemical Property of trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium

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Technology Process of trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium

There total 2 articles about trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 189276-38-8
fluoro(2-iodophenoxymethyl)dimethylsilane

: 183314-77-4
Pd((C₆H₅CHCH)2CO)(As(C₆H₅)3)2

: 189276-42-4
((C₆H₅)3As)2IPd(C₆H₄OCH₂Si(CH₃)2F)

Guidance literature:: In acetone; 23°C;
DOI:10.1021/om970085l

Reference yield: 59.0%

: 189276-38-8
fluoro(2-iodophenoxymethyl)dimethylsilane

: [Pd₂(dibenzylideneacetone)3]*dibenzylideneacetone

: 603-32-7
triphenyl-arsane

: 189276-42-4
trans-bis(triphenylarsine)[2-(fluorodimethylsilylmethoxy)phenyl]iodopalladium

Guidance literature:: In acetone; Ar-atmosphere; stirring soln. of excess of AsPh3 and Pd-complex at 23°C for 3 h, addn. of silane, stirring at 23°C for 24 h; evapn., trituration (Et2O); elem. anal.;
DOI:10.1021/om980157o