1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

Base Information

Chemical Name:1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester
CAS No.:1382486-34-1
Molecular Formula:C₁₆H₁₃BrN₄O₂
Molecular Weight:373.209
Hs Code.:

Synonyms:1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

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Chemical Property of 1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

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Technology Process of 1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

There total 3 articles about 1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(4-bromophenyl)cyclobutane-1-carboxylic acid

: 200731-31-3,148893-10-1
HATU

: 1382486-34-1
1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 1382486-34-1
1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

1.2: 0 - 20 °C

2.1: potassium hydroxide / ethanol / 48 h / 110 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 485828-58-8
1-(4- bromophenyl)cyclobutane-1-carbonitrile

: 1382486-34-1
1-(4-bromophenyl)cyclobutanecarboxylic acid 1,2,3-triazolo[4,5-b]pyridin-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 48 h / 110 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

With N-ethyl-N,N-diisopropylamine; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;