2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

Base Information

Chemical Name:2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane
CAS No.:1429525-70-1
Molecular Formula:C₂₆H₂₄BOPS₃
Molecular Weight:490.459
Hs Code.:

Synonyms:2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

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Chemical Property of 2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

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Technology Process of 2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

There total 3 articles about 2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₁₈OPS₃^(1-)*K⁽¹⁺⁾

: 74-88-4
methyl iodide

: 1429525-70-1
2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

Guidance literature:: C₂₅H₁₈OPS₃^(1-)*K⁽¹⁺⁾; methyl iodide; In tetrahydrofuran; diethylene glycol dimethyl ether; at -20 - 20 ℃; for 0.75h;

With dimethylsulfide borane complex; In tetrahydrofuran; diethylene glycol dimethyl ether; at 0 ℃; for 0.5h;
DOI:10.1016/j.jorganchem.2012.08.032

Reference yield:

: 98-88-4
benzoyl chloride

: 1429525-70-1
2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylene glycol dimethyl ether / 0.25 h / -70 - 20 °C

1.2: 0.5 h / 40 °C

2.1: diethylene glycol dimethyl ether; tetrahydrofuran / 0.75 h / -20 - 20 °C

2.2: 0.5 h / 0 °C

In tetrahydrofuran; diethylene glycol dimethyl ether;
DOI:10.1016/j.jorganchem.2012.08.032

Reference yield:

: C₁₈H₁₄PS₃^(1-)*K⁽¹⁺⁾

: 1429525-70-1
2-(terthienyl)-5-benzoyl-1,3,4-trimethylphosphol-2-enen borane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylene glycol dimethyl ether / 0.25 h / -70 - 20 °C

1.2: 0.5 h / 40 °C

2.1: diethylene glycol dimethyl ether; tetrahydrofuran / 0.75 h / -20 - 20 °C

2.2: 0.5 h / 0 °C

In tetrahydrofuran; diethylene glycol dimethyl ether;
DOI:10.1016/j.jorganchem.2012.08.032