11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

Base Information

Chemical Name:11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid
CAS No.:214051-93-1
Molecular Formula:C₄₁H₄₅N₃O₈
Molecular Weight:707.824
Hs Code.:

Synonyms:11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

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Chemical Property of 11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

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Technology Process of 11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

There total 5 articles about 11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: CHCl₃MeOH

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 214051-92-0
2(S)-Amino-11-[(benzyloxycarbonyl)amino]7-(carbobenzyloxy)-7-azaundecanoic Acid

: 214051-93-1
11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

Guidance literature:: In sodium carbonate; N,N-dimethyl-formamide;

Reference yield: 58.0%

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 214051-92-0
2(S)-Amino-11-[(benzyloxycarbonyl)amino]7-(carbobenzyloxy)-7-azaundecanoic Acid

: 214051-93-1
11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; for 21h; Ambient temperature;
DOI:10.1021/jm980389p

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 214051-93-1
11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2(S)-[(9-fluorenylmethoxycarbonyl)amino]-7-azaundecanoic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / aq. KHCO₃ / diethyl ether / 4 h / Ambient temperature

2: 67 percent / trifluoroacetic acid, triethylsilane / CH₂Cl₂ / 23 h / Ambient temperature

3: 58 percent / 9percent aq. Na₂CO₃ / dimethylformamide / 21 h / Ambient temperature

With triethylsilane; sodium carbonate; potassium hydrogencarbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980389p