N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide

Base Information

• Chemical Name: N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide
• CAS No.: 1293389-49-7
• Molecular Formula: C₁₃H₁₃N₅OS
• Molecular Weight: 287.345
• Mol file: 1293389-49-7.mol

Synonyms:N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide

Chemical Property of N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide

There total 1 articles about N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(2-pyridyl)-3-thiosemicarbazide (36273-89-9) + phenyl isocyanate (103-71-9) → N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide (1293389-49-7)

Guidance literature:

In ethanol; Heating;

DOI:10.1016/j.molstruc.2011.08.020

Reference yield: 90.0%

cobalt(II) chloride hexahydrate + N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide (1293389-49-7) → [Co(N-phenyl-2-(pyridin-2-ylcarbamothioyl)hydrazinecarboxamide)Cl(H2O)2]*H2O

Guidance literature:

In ethanol; soln. was refluxed for 2-3 h; ppt. was filtered off, washed with EtOH and Et2O, dried in vac. over CaCl2; elem. anal.;

DOI:10.1016/j.molstruc.2011.08.020

upstream raw materials:

4-(2-pyridyl)-3-thiosemicarbazide

phenyl isocyanate