(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

Base Information

Chemical Name:(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one
CAS No.:21683-08-9
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

Synonyms:(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

Suppliers and Price of (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

There total 1 articles about (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-92-2,25104-37-4
ethyl vinyl ether

: <4R>-N-(1-methyl-4-isopropenyl)-2-cyclohexylidene-1-phenylethylamine

: 116499-64-0
(R)-dihydrocarvone

: 473-08-5
eudesma-4,11-dien-3-one

: 21683-08-9
(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

Guidance literature:: With sodium methylate; acetic acid; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jo9602534

Reference yield:

: 101671-00-5,5153-68-4
(E)-2-(4-methylphenyl)-1-nitroethene

: 21683-08-9
(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

: C₂₁H₂₈O₂

: C₂₁H₂₈O₂

Guidance literature:: (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one; With ozone; In methanol; at -78 ℃;

(E)-2-(4-methylphenyl)-1-nitroethene; With ferrous(II) sulfate heptahydrate; In methanol; at 0 ℃; Overall yield = 70 percent; Overall yield = 100.4 mg; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.202005267

Reference yield:

: 21683-08-9
(1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one

: 882-33-7
diphenyldisulfane

: C₁₈H₂₄O₂S

: C₁₈H₂₄O₂S

Guidance literature:: (1R,4aR,7R,8aR)-8a-hydroxy-1,4a-dimethyl-7-(prop-1-en-2-yl)-octahydronaphthalen-2(1H)-one; With methanol; ozone;

diphenyldisulfane; With ferrous(II) sulfate heptahydrate; at -78 - 20 ℃; for 0.5h; Overall yield = 40 %; diastereoselective reaction;
DOI:10.1126/science.aaw4212