(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

Base Information

Chemical Name:(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff
CAS No.:108142-72-9
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

Suppliers and Price of (S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

There total 1 articles about (S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 79881-89-3
3-(3-Acetyl-4-hydroxy-phenyl)-1,1-diethylharnstoff

: 23788-74-1,7305-59-1
(R)-2,2-dimethyl-1,3-dioxolane-4-ylmethyl p-toluenesulfonate

: 108142-72-9
(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 50 - 60 ℃; for 2h;

Reference yield:

: 108142-72-9
(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

: 108142-73-0
(R)-3-<3-Acetyl-4-(2,3-dihydroxy-propoxy)-phenyl>-1,1-diethylharnstoff

Guidance literature:: With hydrogenchloride; In acetone; at 60 - 70 ℃; for 0.5h; Yield given;

Reference yield:

: 108142-72-9
(S)-3-<3-Acetyl-4-(2,2-dimethyl-1,3-dioxolan-4-yl-methoxy)-phenyl>-1,1-diethylharnstoff

: (R)-(+)-Celiprolol

Guidance literature:: Multi-step reaction with 4 steps

1: 0.1 N HCl / acetone / 0.5 h / 60 - 70 °C

2: pyridine / 3 h / Ambient temperature

3: Na / methanol / 0.25 h / Ambient temperature

4: 300 mg / 72 h / Ambient temperature

With pyridine; hydrogenchloride; sodium; In methanol; acetone;