1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

Base Information

Chemical Name:1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate
CAS No.:1268593-74-3
Molecular Formula:C₁₉H₃₂O₃SSi
Molecular Weight:368.613
Hs Code.:

Synonyms:1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

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Chemical Property of 1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

Chemical Property:

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Technology Process of 1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

There total 2 articles about 1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(1-hydroxy-1-methylethyl)-3,5-bis[(tert-butyl)dimethylsilanyloxymethyl]benzene

: 507-09-5
tiolacetic acid

: 1268593-74-3
1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

Guidance literature:: With zinc(II) iodide; In 1,2-dichloro-ethane; at 50 ℃; for 0.666667h;

Reference yield:

: 181225-40-1
[[(5-bromo-1,3-phenylene)bis(methylene)]bis(oxy)]bis(tert-butyldimethylsilane)

: 1268593-74-3
1-{3-[(tert-butyl)dimethylsilanyloxymethyl]-5-(hydroxymethyl)phenyl}-1-methylethyl thioacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1.5 h / -71 °C

1.3: 20 °C

2.1: zinc(II) iodide / 1,2-dichloro-ethane / 0.67 h / 50 °C

With n-butyllithium; zinc(II) iodide; In tetrahydrofuran; hexane; 1,2-dichloro-ethane;