diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

Base Information

Chemical Name:diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate
CAS No.:93514-81-9
Molecular Formula:C₁₅H₁₅ClF₃NO₄
Molecular Weight:365.737
Hs Code.:

Synonyms:diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

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Chemical Property of diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

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Technology Process of diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

There total 1 articles about diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 121-50-6
3-amino-4-chlorobenzotrifluoride

: 93514-81-9
diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

Guidance literature:: In toluene; at 140 ℃; for 4h; Inert atmosphere;

Reference yield:

: 93514-81-9
diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

: 64-17-5
ethanol

: 1221573-17-6,93514-85-3
ethyl 8-chloro-4-oxo-5-(trifluoromethyl)-1,4-dihydroquinoline-3-carboxylate

Guidance literature:: With Dowtherm; at 260 ℃; for 6.5h; Product distribution / selectivity;

Reference yield:

: 93514-81-9
diethyl 2-((2-chloro-5-(trifluoromethyl)phenylamino)methylene)malonate

: 1159590-65-4,56881-18-6
ethyl 4-oxo-5-(trifluoromethyl)-1,4-dihydroquinoline-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Dowtherm_.(R). / 6.5 h / 260 °C

2: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol / 20 h / 5 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In ethanol;