methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

Base Information

Chemical Name:methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside
CAS No.:219661-89-9
Molecular Formula:C₂₄H₂₆N₂O₅S
Molecular Weight:454.547
Hs Code.:

Synonyms:methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

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Chemical Property of methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

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Technology Process of methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

There total 5 articles about methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 102339-30-0
(3R,4R,5R)-4-(benzyloxy)-5-(benzyloxymethyl)-2-methoxytetrahydrofuran-3-ol

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 219661-89-9
methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

Guidance literature:: In 1,2-dichloro-ethane; for 3h; Heating;
DOI:10.1080/07328319808004318

Reference yield:

: 100-39-0
benzyl bromide

: 219661-89-9
methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / KOH / tetrahydrofuran / 24 h / Heating

2: aq. CF₃COOH / 3 h / 0 °C

3: 90 percent / conc. H₂SO₄ / 24 h / 0 °C

4: 88 percent / 1,2-dichloro-ethane / 3 h / Heating

With potassium hydroxide; sulfuric acid; trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1080/07328319808004318

Reference yield:

: 41341-99-5
3,5-di-O-benzyl-1,2-O-isopropylidene-α-D-xylofuranose

: 219661-89-9
methyl 2-deoxy-3,5-di-O-benzyl-2-(1-imidazoyl)thiocarbonyloxy-D-xylofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: aq. CF₃COOH / 3 h / 0 °C

2: 90 percent / conc. H₂SO₄ / 24 h / 0 °C

3: 88 percent / 1,2-dichloro-ethane / 3 h / Heating

With sulfuric acid; trifluoroacetic acid; In 1,2-dichloro-ethane;
DOI:10.1080/07328319808004318