3,5-Dibromo-4-methoxybenzonitrile

Base Information

Chemical Name:3,5-Dibromo-4-methoxybenzonitrile
CAS No.:3336-39-8
Molecular Formula:C8H5 Br2 N O
Molecular Weight:290.94
Hs Code.:2926909090
DSSTox Substance ID:DTXSID40372470
Nikkaji Number:J265.505E
Wikidata:Q82160196
Mol file:3336-39-8.mol

Synonyms:3,5-dibromo-4-methoxybenzonitrile;3336-39-8;Bromoxynil-methyl ether;Bromoxynil methyl ether;BROMOXYNIL-METHYLETHER;Maybridge1_008600;SCHEMBL7627302;HMS565O20;DTXSID40372470;BUGMOVRSBPGSOS-UHFFFAOYSA-N;3,5-Dibromo-4-methoxy-benzonitrile;CCG-50775;MFCD00017333;AKOS002391621;BB 0246985;CS-0377850;FT-0614500;J-019160;SR-01000640124-1

Suppliers and Price of 3,5-Dibromo-4-methoxybenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
BromoxynilMethylEther
500mg
$ 55.00

Biosynth Carbosynth
3,5-Dibromo-4-methoxybenzonitrile
50 g
$ 300.00

Biosynth Carbosynth
3,5-Dibromo-4-methoxybenzonitrile
25 g
$ 200.00

Biosynth Carbosynth
3,5-Dibromo-4-methoxybenzonitrile
10 g
$ 100.00

Biosynth Carbosynth
3,5-Dibromo-4-methoxybenzonitrile
5 g
$ 55.00

American Custom Chemicals Corporation
BROMOXYNIL-METHYL ETHER 95.00%
25G
$ 1619.03

AHH
3,5-Dibromo-4-methoxybenzonitrile 97%
25g
$ 435.00

Total 11 raw suppliers

Chemical Property of 3,5-Dibromo-4-methoxybenzonitrile

Chemical Property:

Vapor Pressure:0.000658mmHg at 25°C
Melting Point:115-117°C
Boiling Point:309°Cat760mmHg
Flash Point:140.7°C
PSA：33.02000
Density:1.95g/cm³
LogP:3.09188
Storage Temp.:APPROX 4°C
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:290.87174
Heavy Atom Count:12
Complexity:189

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

BromoxynilMethylEther ^*data from reagent suppliers

Safty Information:

Pictogram(s): F,Xn,N
Hazard Codes:F,Xn,N,T+
Statements: 36/37/38-67-65-50/53-38-11-43-26-25-63
Safety Statements: 26-36/37/39-61-60-33-16-63-45-36/37-28-27

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)C#N)Br
Uses Bromoxynil Methyl Ether is used in preparation of 2,5''-Disubstituted bibenzimidazoles related to Hoechst 33258.

Technology Process of 3,5-Dibromo-4-methoxybenzonitrile

There total 1 articles about 3,5-Dibromo-4-methoxybenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3336-39-8
3,5-dibromo-4-methoxybenzonitrile

Guidance literature:: aus 3,5-Dibrom-4-methoxybenzamid;

Reference yield: 93.0%

: 64-17-5
ethanol

: 3336-39-8
3,5-dibromo-4-methoxybenzonitrile

: 3,5-dibromo-4-methoxybenzenecarboximidic acid ethyl ester monohydrochloride

Guidance literature:: With hydrogenchloride; In ethanol;

Reference yield:

: 3336-39-8
3,5-dibromo-4-methoxybenzonitrile

: 1026715-13-8
2-(3,5-Dibromo-4-methoxy-phenyl)-1-(4-methanesulfonyl-phenyl)-4-trifluoromethyl-4,5-dihydro-1H-imidazol-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylaluminum / 1.) toluene, a) 0 deg C - RT, b) RT, 3.5 h, 2.) toluene, 70 deg C - 75 deg C, 17 h

2: sodium hydrogencarbonate / isopropyl alcohol / 20 h / 75 - 80 °C

With trimethylaluminum; sodium hydrogencarbonate; In isopropyl alcohol;
DOI:10.1021/jm9700225