C₃₄H₃₄O₆

Base Information

• Chemical Name: C₃₄H₃₄O₆
• CAS No.: 1332848-96-0
• Molecular Formula: C₃₄H₃₄O₆
• Molecular Weight: 538.64
• Mol file: 1332848-96-0.mol

Synonyms:C₃₄H₃₄O₆

Chemical Property of C₃₄H₃₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₄O₆

There total 7 articles about C₃₄H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C38H42O6 (1332849-09-8) → C34H34O6 (1332848-96-0)

Guidance literature:

C₃₈H₄₂O₆; With potassium hydroxide; In tetrahydrofuran; ethanol; at 20 ℃; for 13h;

With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1002/chem.201101015

Reference yield:

1-Bromopentane (110-53-2) → C34H34O6 (1332848-96-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 17.5 h / 60 °C / Inert atmosphere

2.1: sulfuric acid; iodine; periodic acid / dichloromethane; water; acetic acid / 16.5 h / 75 °C

3.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

4.1: potassium hydroxide / tetrahydrofuran; ethanol / 13 h / 20 °C

4.2: 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; iodine; potassium carbonate; periodic acid; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;

DOI:10.1002/chem.201101015

Reference yield:

1,4-di(n-pentyloxy)benzene (32527-64-3) → C34H34O6 (1332848-96-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sulfuric acid; iodine; periodic acid / dichloromethane; water; acetic acid / 16.5 h / 75 °C

2.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

3.1: potassium hydroxide / tetrahydrofuran; ethanol / 13 h / 20 °C

3.2: 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; iodine; periodic acid; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; acetic acid;

DOI:10.1002/chem.201101015

upstream raw materials:

1,4-diiodo-2,5-dipentoxybenzene

ethyl 4-ethynylbenzoate

C₃₈H₄₂O₆

1-Bromopentane