1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane

Base Information

• Chemical Name: 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane
• CAS No.: 110698-83-4
• Molecular Formula: C₃₆H₄₄OSi₂
• Molecular Weight: 548.916

Synonyms:1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane

Chemical Property of 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane

Chemical Property:

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Technology Process of 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane

There total 11 articles about 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

tetramesityldisilene (80785-72-4) → 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane (110698-83-4) + C42H54OSi2

Guidance literature:

With cyclohexane-1,2-epoxide; at 80 ℃; for 168h;

DOI:10.1039/c39930001348

Reference yield: 45.0%

cyclohexane-1,2-epoxide (286-20-4) + tetramesityldisilene (80785-72-4) → 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane (110698-83-4) + C42H54OSi2

Guidance literature:

at 80 ℃; for 168h;

DOI:10.1039/c39930001348

Reference yield: 18.9%

tetramesityldisilene (80785-72-4) + methyloxirane (75-56-9,16033-71-9) → 1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane (110698-83-4) + 4-Methyl-2,2,3,3-tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,3]oxadisilolane + C39H50OSi2 + C39H50OSi2

Guidance literature:

In benzene; Yields of byproduct given; Heating;

DOI:10.1016/0022-328X(95)06069-9

upstream raw materials:

cyclohexane-1,2-epoxide

tetramesityldisilene

2-methyl-1,2-epoxypropane

1,2-epoxy-3,3-dimethylbutane

Downstream raw materials:

1,1,3,3-tetramesityl-1,3-cyclodisiloxane

3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane

2-(2,4,6-Trimethyl-phenoxy)-2,4,4-tris-(2,4,6-trimethyl-phenyl)-[1,3,2,4]dioxadisiletane

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