3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane

Base Information

• Chemical Name: 3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane
• CAS No.: 130481-31-1
• Molecular Formula: C₃₆H₄₄O₃Si₂
• Molecular Weight: 580.915
• Mol file: 130481-31-1.mol

Synonyms:3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane

Chemical Property of 3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane

There total 1 articles about 3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane (110698-83-4) → 1,1,3,3-tetramesityl-1,3-cyclodisiloxane (84537-22-4) + 3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane (130481-31-1)

Guidance literature:

With oxygen; 5,15,10,20-tetraphenylporphyrin; In benzene; Yield given. Yields of byproduct given; Ambient temperature; Irradiation;

DOI:10.1016/S0040-4039(00)97575-0

Reference yield: 94.0%

3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane (130481-31-1) → 2-(2,4,6-Trimethyl-phenoxy)-2,4,4-tris-(2,4,6-trimethyl-phenyl)-[1,3,2,4]dioxadisiletane (130481-33-3)

Guidance literature:

In toluene; at 100 ℃;

DOI:10.1016/S0040-4039(00)97575-0

Reference yield: 83.0%

3,3,5,5-Tetrakis-(2,4,6-trimethyl-phenyl)-[1,2,4,3,5]trioxadisilolane (130481-31-1) → 1,1,3,3-tetramesityl-1,3-cyclodisiloxane (84537-22-4)

Guidance literature:

With triphenylphosphine; Ambient temperature;

DOI:10.1016/S0040-4039(00)97575-0

upstream raw materials:

1,1,2,2-tetramesityl-3-oxa-1,2-disilacyclopropane

Downstream raw materials:

1,1,3,3-tetramesityl-1,3-cyclodisiloxane

2-(2,4,6-Trimethyl-phenoxy)-2,4,4-tris-(2,4,6-trimethyl-phenyl)-[1,3,2,4]dioxadisiletane