3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Base Information

Chemical Name:3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin
CAS No.:1332462-84-6
Molecular Formula:C₁₇H₁₁ClN₆O₄
Molecular Weight:398.765
Hs Code.:

Synonyms:3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

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Chemical Property of 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

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Technology Process of 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

There total 4 articles about 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 611-09-6
5-nitroisatin

: 147440-65-1
4-amino-3-(p-chlorobenzyl)-1H-1,2,4-triazol-5-one

: 1332462-84-6
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: With acetic acid; In ethanol; at 110 ℃; for 0.05h; Microwave irradiation; Closed vessel;
DOI:10.3184/174751911X13043524455143

Reference yield:

: 17122-62-2
hydroxyimino-acetic acid-(4-nitro-anilide)

: 1332462-84-6
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: acetic acid / ethanol / 0.05 h / 110 °C / Microwave irradiation; Closed vessel

With acetic acid; In ethanol;
DOI:10.3184/174751911X13043524455143

Reference yield:

: 141525-15-7
ethyl 2-[2-(4-chlorophenyl)-1-ethoxyethylidene]hydrazinecarboxylate

: 1332462-84-6
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water / 0.05 h / 90 °C / Microwave irradiation; Closed vessel

2: acetic acid / ethanol / 0.05 h / 110 °C / Microwave irradiation; Closed vessel

With hydrazine hydrate; acetic acid; In ethanol; water;
DOI:10.3184/174751911X13043524455143