2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

Base Information

Chemical Name:2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde
CAS No.:1194283-39-0
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

Synonyms:2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

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Chemical Property of 2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

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Technology Process of 2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

There total 1 articles about 2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1745-07-9
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

: 71924-62-4
2-fluoro-4,5-dimethoxybenzaldehyde

: 1194283-39-0
2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 23h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201103155

Reference yield: 92.0%

: 19615-20-4
1-amino-2-phenylaziridine

: 1194283-39-0
2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

: 1361538-07-9
N-(2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzylidene)-2-phenylaziridin-1-amine

Guidance literature:: In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201103155

Reference yield:

: 1194283-39-0
2-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)-4,5-dimethoxybenzaldehyde

: 58939-41-6
O-methylcryptaustoline iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 20 °C / Inert atmosphere

2.1: dirhodium(II) tetrakis(methyl 2-oxopyrrolidine-5(S)-carboxylate) / toluene / 6 h / 100 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With dirhodium(II) tetrakis(methyl 2-oxopyrrolidine-5(S)-carboxylate); In ethanol; toluene;
DOI:10.1002/chem.201103155