N-(4-fluorophenyl)selenocarbamate of cholestanol

Base Information

Chemical Name:N-(4-fluorophenyl)selenocarbamate of cholestanol
CAS No.:154592-72-0
Molecular Formula:C₃₄H₅₂FNOSe
Molecular Weight:588.751
Hs Code.:

Synonyms:N-(4-fluorophenyl)selenocarbamate of cholestanol

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Chemical Property of N-(4-fluorophenyl)selenocarbamate of cholestanol

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Technology Process of N-(4-fluorophenyl)selenocarbamate of cholestanol

There total 4 articles about N-(4-fluorophenyl)selenocarbamate of cholestanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 80-97-7
Cholestanol

: 154592-60-6
1-fluoro-4-isoselenocyanatobenzene

: 154592-72-0
N-(4-fluorophenyl)selenocarbamate of cholestanol

Guidance literature:: With potassium hydride; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80783-3

Reference yield:

: 459-25-6
N-(4-fluorophenyl)formamide

: 154592-72-0
N-(4-fluorophenyl)selenocarbamate of cholestanol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Ph₃P, Et₃N / CCl₄ / 70 °C

2: 70 percent / Se (powder), Et₃N

3: 70 percent / potassium hydride / tetrahydrofuran / 4 h / Ambient temperature

With selenium; potassium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4020(01)80783-3

Reference yield:

: 371-40-4
4-fluoroaniline

: 154592-72-0
N-(4-fluorophenyl)selenocarbamate of cholestanol

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 12 h / Heating

2: 88 percent / Ph₃P, Et₃N / CCl₄ / 70 °C

3: 70 percent / Se (powder), Et₃N

4: 70 percent / potassium hydride / tetrahydrofuran / 4 h / Ambient temperature

With selenium; potassium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4020(01)80783-3