1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside

Base Information

Chemical Name:1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside
CAS No.:145416-95-1
Molecular Formula:C₁₇H₂₂Cl₃NO₁₁
Molecular Weight:522.721
Hs Code.:

Synonyms:1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside

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Chemical Property of 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside

There total 8 articles about 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2',2',2'-trichloroethoxycarbonylamino)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 172490-46-9
2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranose

: 122210-01-9,122210-05-3,145416-95-1,146864-65-5,114360-77-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranose

Guidance literature:: In pyridine; at 20 ℃; for 12h;
DOI:10.1021/ja302099u

Reference yield: 92.0%

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 108-24-7
acetic anhydride

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 122210-01-9,122210-05-3,145416-95-1,146864-65-5,114360-77-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranose

Guidance literature:: (+)-D-glucosamine hydrochloride; 2,2,2-Trichloroethyl chloroformate; With sodium hydrogencarbonate; In water; at 20 ℃; for 1h;

acetic anhydride; With pyridine; at 20 ℃;
DOI:10.1093/glycob/cwx017

Reference yield: 87.0%

: 114297-26-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 122210-01-9,122210-05-3,145416-95-1,146864-65-5,114360-77-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranose

Guidance literature:: 1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose; With hydrogenchloride; water; In acetone; Reflux;

2,2,2-Trichloroethyl chloroformate; With pyridine; at 0 ℃; for 3h;