methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

Base Information

Chemical Name:methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate
CAS No.:1373340-57-8
Molecular Formula:C₂₀H₁₇NO₄
Molecular Weight:335.359
Hs Code.:

Synonyms:methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

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Chemical Property of methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

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Technology Process of methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

There total 1 articles about methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942-24-5
3-methoxycarbonylindole

: 154884-62-5
3-(2-methoxyphenyl)propargyl alcohol

: 1373340-57-8
methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

Guidance literature:: 3-methoxycarbonylindole; With N,N'-dimethylpiperazine; N-chloro-succinimide; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;

3-(2-methoxy-phenyl)-prop-2-yn-1-ol; With trichloroacetic acid; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201107417

Reference yield: 90.0%

: 1373340-57-8
methyl 2-((3-(2-methoxyphenyl)prop-2-yn-1-yl)oxy)-1H-indole-3-carboxylate

: 1373340-31-8
(S)-methyl 3-(1-(2-methoxyphenyl)propa-1,2-dien-1-yl)-2-oxoindoline-3-carboxylate

Guidance literature:: With Pd[(S)-t-BuPHOX](SbF₆)2; In dichloromethane; at -78 - -15 ℃; for 8h; optical yield given as %ee; enantioselective reaction; Darkness; Inert atmosphere;
DOI:10.1002/anie.201107417