5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole

Base Information

• Chemical Name: 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole
• CAS No.: 1357066-27-3
• Molecular Formula: C₄₂H₃₀N₄
• Molecular Weight: 590.727
• Mol file: 1357066-27-3.mol

Synonyms:5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole

Chemical Property of 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole

There total 7 articles about 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene (1257220-47-5) + 2-(4-bromobenzenyl)-4,6-diphenyl-1,3,5-triazine (23449-08-3) → 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole (1357066-27-3)

Guidance literature:

With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane; In toluene; at 100 ℃; Inert atmosphere;

DOI:10.1016/j.dyepig.2019.107650

Reference yield: 85.0%

→ 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole (1357066-27-3)

Guidance literature:

With tri-tert-butyl phosphine; palladium diacetate; In para-xylene; for 16h; Reflux;

Reference yield: 30.0%

2-chloro-4,6-diphenyl-1,3,5-triazine (3842-55-5) + C27H22BNO2 (1357066-50-2) → 5-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-7,7-dimethyl-5,7-dihydroindeno[2,1-b]carbazole (1357066-27-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 120 ℃; for 12h;

upstream raw materials:

12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

10-(4-Bromophenyl)-12,12-dimethyl-10,12dihydro-10-azaindeno[2,1-b]-fluorene

2-chloro-4,6-diphenyl-1,3,5-triazine

C₂₇H₂₂BNO₂