Technology Process of C33H43N7O3
There total 9 articles about C33H43N7O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hypochlorite; sodium hydrogencarbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 4 h / 0 - 20 °C
2.1: dichloromethane / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: hydrogen / palladium(II) hydroxide/carbon / ethanol / 48 h / 20 °C / 760.05 Torr
4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C
With
sodium hypochlorite; hydrogen; sodium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium(II) hydroxide/carbon;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; N,N`-dimethylethylenediamine / copper(l) iodide / 1,4-dioxane / 16 h / 110 °C
2.1: potassium hydroxide / ethanol; water / 24 h / 40 °C
2.2: pH 4
3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C
With
potassium hydroxide; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine;
copper(l) iodide;
In
1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;