C₂₆H₂₉O₃P

Base Information

• Chemical Name: C₂₆H₂₉O₃P
• CAS No.: 1373432-13-3
• Molecular Formula: C₂₆H₂₉O₃P
• Molecular Weight: 420.488

Synonyms:C₂₆H₂₉O₃P

Chemical Property of C₂₆H₂₉O₃P

Chemical Property:

Purity/Quality:

97% purity >99% ee ^*data from raw suppliers

(2S,3S)-2-Benzyl-3-(tert-butyl)-4-(2,6-dimethoxyphenyl)-2,3-dihydrobenzo[d][1,3]oxaphosphole, 97% (>99% ee) ^*data from reagent suppliers

Safty Information:

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Technology Process of C₂₆H₂₉O₃P

There total 4 articles about C₂₆H₂₉O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(2S,3R)-2-benzyl-3-tert-butyl-4-(2,6-dimethoxyphenyl)-2,3-dihydrobenzo[d][1,3]oxaphosphole oxide (1373432-38-2) → C26H29O3P (1373432-13-3)

Guidance literature:

With titanium(IV) isopropylate; In tetrahydrofuran; for 24h; stereospecific reaction; Reflux; Inert atmosphere;

DOI:10.1021/ol300659d

Reference yield:

(R)-3-(tert-butyl)-3-oxido-2H-benzo[d][1,3]oxaphosphol-4-yl trifluoromethanesulfonate (1202032-99-2) → C26H29O3P (1373432-13-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride / 1,4-dioxane / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

2.2: 3 h / -70 - 20 °C / Inert atmosphere

3.1: titanium(IV) isopropylate / tetrahydrofuran / 24 h / Reflux; Inert atmosphere

With titanium(IV) isopropylate; potassium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; 1.1: Suzuki coupling;

DOI:10.1021/ol300659d

Reference yield:

(2,6-dimethoxyphenyl)boronic acid (23112-96-1) → C26H29O3P (1373432-13-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride / 1,4-dioxane / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

2.2: 3 h / -70 - 20 °C / Inert atmosphere

3.1: titanium(IV) isopropylate / tetrahydrofuran / 24 h / Reflux; Inert atmosphere

With titanium(IV) isopropylate; potassium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; 1.1: Suzuki coupling;

DOI:10.1021/ol300659d

upstream raw materials:

(R)-3-(tert-butyl)-3-oxido-2H-benzo[d][1,3]oxaphosphol-4-yl trifluoromethanesulfonate

(R)-3-(tert-butyl)-4-(2,6-dimethoxyphenyl)-2,3 dihydrobenzo[d][1,3]oxaphosphole-3-oxide

benzyl bromide

(2S,3R)-2-benzyl-3-tert-butyl-4-(2,6-dimethoxyphenyl)-2,3-dihydrobenzo[d][1,3]oxaphosphole oxide

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