methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

Base Information

Chemical Name:methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose
CAS No.:20702-73-2
Molecular Formula:C₁₅H₁₈O₅
Molecular Weight:278.305
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

Suppliers and Price of methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

There total 5 articles about methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5987-36-0
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside

: 20702-73-2
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

Guidance literature:: With dimethyl sulfoxide; trifluoroacetic anhydride; In dichloromethane; at -65 ℃; for 0.75h;

Reference yield:

: 5987-36-0
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside

: 20702-73-2
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

: 77516-58-6
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

Guidance literature:: methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside; With trifluoroacetic anhydride; In dichloromethane; at -65 ℃; for 1h;

With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at -65 - 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2007.02.024

Reference yield:

: 3150-16-1
methyl 4,6-O-benzylidene-2,3-anhydro-α-D-mannopyranoside

: 20702-73-2
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether; tetrahydrofuran / 17 h / Heating

2.1: (CF₃CO)2O / CH₂Cl₂ / 1 h / -65 °C

2.2: triethylamine / CH₂Cl₂; dimethylformamide / -65 - 20 °C

With trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2007.02.024