methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

Base Information

Chemical Name:methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose
CAS No.:77516-58-6
Molecular Formula:C₁₅H₁₈O₅
Molecular Weight:278.305
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

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Technology Process of methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

There total 9 articles about methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 20702-73-2
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

: 77516-58-6
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 36h; Ambient temperature;

Reference yield:

: 5987-36-0
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside

: 77516-58-6
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; Yield given. Multistep reaction; 1.) DMSO, pyridine, benzene, RT, 7h, 2.) DMF, RT, 3d;
DOI:10.1246/bcsj.53.3252

Reference yield:

: 5987-36-0
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside

: 20702-73-2
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-ribo-hexopyranosid-2-ulose

: 77516-58-6
methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-L-arabino-hexopyranosid-2-ulose

Guidance literature:: methyl 4,6-O-benzylidene-3-deoxy-3-C-methyl-α-D-altropyranoside; With trifluoroacetic anhydride; In dichloromethane; at -65 ℃; for 1h;

With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at -65 - 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2007.02.024