3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

Base Information

Chemical Name:3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate
CAS No.:1017234-25-1
Molecular Formula:C₂₁H₂₈N₂O₂
Molecular Weight:340.466
Hs Code.:

Synonyms:3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

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Chemical Property of 3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

Chemical Property:

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Technology Process of 3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

There total 4 articles about 3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42252-34-6
N-ethyl-N-methylcarbamoyl chloride

: 1017234-23-9
(1S)-N-((S)-1-(3-hydroxyphenyl)ethyl)-N-methyl-1-phenylethanamine

: 1017234-25-1
3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

Guidance literature:: (1S)-N-((S)-1-(3-hydroxyphenyl)ethyl)-N-methyl-1-phenylethanamine; With sodium hydride; In tetrahydrofuran; mineral oil; Inert atmosphere;

N-ethyl-N-methylcarbamoyl chloride; In tetrahydrofuran; mineral oil; for 4h; Inert atmosphere;
DOI:10.1080/00397910802531948

Reference yield:

: 855300-09-3
1-(N-ethyl-N-methylaminocarbonyloxy)-3-acetylbenzene

: 1017234-25-1
3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 56 h / 130 °C / Dean-Stark; Molecular sieve; Flow reactor

2.1: trichlorosilane; N,N-dimethyl-formamide / dichloromethane / 18 h / -20 °C / Inert atmosphere

2.2: 0 °C

3.1: formic acid / water / 4 h / Reflux

With formic acid; trichlorosilane; N,N-dimethyl-formamide; In dichloromethane; water; toluene;
DOI:10.1002/ejoc.201601268

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1017234-25-1
3-[(1S)-1-{methyl[(1S)-1-phenylethyl]amino}ethyl]phenyl N-ethyl-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 56 h / 130 °C / Dean-Stark; Molecular sieve; Flow reactor

2.1: trichlorosilane; N,N-dimethyl-formamide / dichloromethane / 18 h / -20 °C / Inert atmosphere

2.2: 0 °C

3.1: formic acid / water / 4 h / Reflux

With formic acid; trichlorosilane; N,N-dimethyl-formamide; In dichloromethane; water; toluene;
DOI:10.1002/ejoc.201601268