N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine
CAS No.:927824-75-7
Molecular Formula:C₃₃H₃₇NO₈
Molecular Weight:575.659
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

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Chemical Property of N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

Chemical Property:

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Technology Process of N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

There total 2 articles about N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 874-60-2
4-methyl-benzoyl chloride

: 146651-71-0
N-(tert-butyloxycarbonyl)-2-amino-2-(hydroxymethyl)propane-1,3-diol

: 927824-75-7
N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

Guidance literature:: With triethylamine; In dichloromethane; for 20h; Heating;
DOI:10.1039/b609500c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 927824-75-7
N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / tetrahydrofuran / 96 h / 20 °C

2: 92 percent / Et₃N / CH₂Cl₂ / 20 h / Heating

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b609500c

Reference yield: 77.0%

: 927824-75-7
N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine

: 1,1,1-tris(4-methylbenzoyloxymethyl)methylamine

Guidance literature:: N-(tert-butyloxycarbonyl)-1,1,1-tris(4-methylbenzoyloxy-methyl)methylamine; In dichloromethane; for 18h; cooling;

With sodium carbonate; In water; Further stages.;
DOI:10.1039/b609500c