[(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

Base Information

Chemical Name:[(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester
CAS No.:114032-15-4
Molecular Formula:C₁₄H₂₄O₃
Molecular Weight:240.343
Hs Code.:

Synonyms:[(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

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Chemical Property of [(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

Chemical Property:

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Technology Process of [(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

There total 6 articles about [(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1184-58-3
dimethylaluminum chloride

: 114032-14-3
((1S,2R,5R)-2-Isopropenyl-5-methyl-cyclohexyl)-acetic acid methyl ester

: 114032-15-4
[(1S,2R,5R)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

Guidance literature:: With formaldehyd; In dichloromethane; at 0 - 20 ℃; for 4h;

Reference yield:

: 5949-05-3
(S)-Citronellal

: 114032-15-4
[(1R,2S,5S)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium acetate / CH₂Cl₂

2: FeCl₃/Al₂O₃

3: NaCl,Me₂SO / H₂O

4: (CH₂O)n / CH₂Cl₂

With aluminum oxide; formaldehyd; pyridinium acetate; iron(III) chloride; dimethyl sulfoxide; sodium chloride; In dichloromethane; water;

Reference yield:

: 130451-44-4
2-((S)-3,7-Dimethyl-oct-6-enylidene)-malonic acid dimethyl ester

: 114032-15-4
[(1R,2S,5S)-2-(3-Hydroxy-1-methylene-propyl)-5-methyl-cyclohexyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: FeCl₃/Al₂O₃

2: NaCl,Me₂SO / H₂O

3: (CH₂O)n / CH₂Cl₂

With aluminum oxide; formaldehyd; iron(III) chloride; dimethyl sulfoxide; sodium chloride; In dichloromethane; water;