(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

Base Information

Chemical Name:(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd
CAS No.:100100-75-2
Molecular Formula:C₁₉H₂₀O₆
Molecular Weight:344.364
Hs Code.:

Synonyms:(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

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Chemical Property of (2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

Chemical Property:

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Technology Process of (2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

There total 3 articles about (2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 100100-74-1
(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-hydroxymethyl-1,4-benzodioxan-6-carbaldehyd

: 74-88-4
methyl iodide

: 100100-75-2
(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

Guidance literature:: With silver(l) oxide; In acetone; at 55 ℃; for 72h;

Reference yield:

: 69506-79-2,76870-73-0,133906-60-2
rac-Americanin-A

: 100100-75-2
(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / K₂CO₃ / acetone / Heating

2: 72 percent / OsO₄, NaIO₄ / dioxane / 12 h / Ambient temperature

3: 73 percent / Ag₂O / acetone / 72 h / 55 °C

With sodium periodate; osmium(VIII) oxide; potassium carbonate; silver(l) oxide; In 1,4-dioxane; acetone;

Reference yield:

: 100100-73-0
rac-Americanin-A dimethylether

: 100100-75-2
(2RS,3RS)-2-(3,4-Dimethoxyphenyl)-3-methoxymethyl-1,4-benzodioxan-6-carbaldehyd

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / OsO₄, NaIO₄ / dioxane / 12 h / Ambient temperature

2: 73 percent / Ag₂O / acetone / 72 h / 55 °C

With sodium periodate; osmium(VIII) oxide; silver(l) oxide; In 1,4-dioxane; acetone;