6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

Base Information

Chemical Name:6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine
CAS No.:909413-26-9
Molecular Formula:C₂₅H₂₈NSb
Molecular Weight:464.254
Hs Code.:

Synonyms:6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

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Chemical Property of 6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

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Technology Process of 6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

There total 3 articles about 6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1070804-80-6
6-(tert-butyl)-12-chloro-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

: 5720-05-8
4-methylphenylboronic acid

: 909413-26-9
6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

Guidance literature:: With water; nickel diacetate; sodium carbonate; In toluene; at 100 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202011491

Reference yield:

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 909413-26-9
6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 120 °C / Schlenk technique; Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / -78 - 20 °C / Inert atmosphere

2.2: 14 h / -78 - 20 °C / Inert atmosphere

3.1: nickel diacetate; sodium carbonate; water / toluene / 12 h / 100 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; water; nickel diacetate; sodium carbonate; potassium carbonate; In diethyl ether; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.202011491

Reference yield:

: 194285-51-3
N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

: 909413-26-9
6-(tert-butyl)-12-(p-tolyl)-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; diethyl ether / -78 - 20 °C / Inert atmosphere

1.2: 14 h / -78 - 20 °C / Inert atmosphere

2.1: nickel diacetate; sodium carbonate; water / toluene / 12 h / 100 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; water; nickel diacetate; sodium carbonate; In diethyl ether; hexane; toluene;
DOI:10.1002/anie.202011491