trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester
CAS No.:1200131-14-1
Molecular Formula:C₁₄H₁₇ClF₃NO₄S
Molecular Weight:387.807
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

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Chemical Property of trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

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Technology Process of trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

There total 3 articles about trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 421-83-0
trifluoromethane sulfonyl chloride

: 1200131-13-0
3-chloro-5-methoxy-4-piperidin-1-ylmethylphenol

: 1200131-14-1
trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

Guidance literature:: With pyridine; In dichloromethane; at -20 - 20 ℃;

Reference yield:

: 110-89-4
piperidine

: 1200131-14-1
trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tris(acetoxy)borohydride / dichloromethane / 0 - 20 °C

1.2: pH 2

1.3: pH 9

2.1: hydrogen iodide / water / 2 h / 60 °C

2.2: 20 °C

3.1: pyridine / dichloromethane / -20 - 20 °C

With pyridine; hydrogen iodide; sodium tris(acetoxy)borohydride; In dichloromethane; water;

Reference yield:

: 82477-61-0
2-chloro-4,6-dimethoxybenzaldehyde

: 1200131-14-1
trifluoromethanesulfonic acid 3-chloro-5-methoxy-4-piperidin-1-ylmethylphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tris(acetoxy)borohydride / dichloromethane / 0 - 20 °C

1.2: pH 2

1.3: pH 9

2.1: hydrogen iodide / water / 2 h / 60 °C

2.2: 20 °C

3.1: pyridine / dichloromethane / -20 - 20 °C

With pyridine; hydrogen iodide; sodium tris(acetoxy)borohydride; In dichloromethane; water;