<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

Base Information

Chemical Name:<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone
CAS No.:117498-51-8
Molecular Formula:C₁₇H₁₇N₃O₇S
Molecular Weight:407.404
Hs Code.:

Synonyms:<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

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Chemical Property of <4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

Chemical Property:

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Technology Process of <4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

There total 5 articles about <4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 528-45-0
3,4-dinitrobenzoic acid

: 117498-51-8
<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 12 h / Heating

2: AlCl₃ / CH₂Cl₂ / 2.5 h / Heating

3: 78 percent / 45percent sulfuric aicd / 4.5 h / Heating

4: thionyl chloride / 3 h / Heating

5: 1.) azidotrimethylsilane / 1.) toluene, reflux, 16 h, 2.) reflux, 6 h

With aluminium trichloride; thionyl chloride; trimethylsilylazide; sulfuric acid; In dichloromethane;
DOI:10.1021/jm00122a020

Reference yield:

: 24376-18-9
3,4-dinitrobenzoyl chloride

: 117498-51-8
<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃ / CH₂Cl₂ / 2.5 h / Heating

2: 78 percent / 45percent sulfuric aicd / 4.5 h / Heating

3: thionyl chloride / 3 h / Heating

4: 1.) azidotrimethylsilane / 1.) toluene, reflux, 16 h, 2.) reflux, 6 h

With aluminium trichloride; thionyl chloride; trimethylsilylazide; sulfuric acid; In dichloromethane;
DOI:10.1021/jm00122a020

Reference yield:

: 117498-47-2
<4-(cyanomethyl)2-thienyl>(3,4-dinitrophenyl)methanone

: 117498-51-8
<4-<<(tert-butoxycarbonyl)amino>methyl>-2-thienyl>(3,4-dinitrophenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 45percent sulfuric aicd / 4.5 h / Heating

2: thionyl chloride / 3 h / Heating

3: 1.) azidotrimethylsilane / 1.) toluene, reflux, 16 h, 2.) reflux, 6 h

With thionyl chloride; trimethylsilylazide; sulfuric acid;
DOI:10.1021/jm00122a020