(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

Base Information

Chemical Name:(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene
CAS No.:1225055-89-9
Molecular Formula:C₂₉H₃₈OSi₂
Molecular Weight:458.791
Hs Code.:

Synonyms:(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

Suppliers and Price of (R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

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Technology Process of (R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

There total 1 articles about (R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246176-15-7
(R)-2-(dimethyl(phenyl)silyl)pent-3-en-1-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1225055-89-9
(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol100604m

Reference yield: 92.0%

: 1825-61-2
Trimethylmethoxysilane

: 1225055-89-9
(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 1225056-16-5
tert-butyl((2E,4S,5R)-5-(2,3-dimethoxyphenyl)-5-methoxy-4-methylpent-2-enyloxy)diphenylsilane

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; optical yield given as %de; diastereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol100604m

Reference yield: 87.0%

: 14642-79-6
benzyloxy-trimethylsilane

: 1225055-89-9
(R,E)-1-((1-(tert-butyldiphenylsilyloxy)pent-3-en-2-yl)dimethylsilyl)benzene

: 93-02-7
2,5-dimethoxybenzaldehyde

: 1225056-23-4
((2E,4S,5R)-5-(benzyloxy)-5-(2,5-dimethoxyphenyl)-4-methylpent-2-enyloxy)(tert-butyl)diphenylsilane

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; optical yield given as %de; diastereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol100604m