C₂₅H₂₂F₃NO₄

Base Information

Chemical Name:C₂₅H₂₂F₃NO₄
CAS No.:916219-96-0
Molecular Formula:C₂₅H₂₂F₃NO₄
Molecular Weight:457.449
Hs Code.:

C<sub>25</sub>H<sub>22</sub>F<sub>3</sub>NO<sub>4</sub>

Synonyms:C₂₅H₂₂F₃NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₂F₃NO₄

Chemical Property:

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Technology Process of C₂₅H₂₂F₃NO₄

There total 4 articles about C₂₅H₂₂F₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 916219-93-7
C₂₅H₂₁F₃O₅

: 916219-96-0
C₂₅H₂₂F₃NO₄

Guidance literature:: With ammonia; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In propan-1-ol; dichloromethane; for 8h; Inert atmosphere;
DOI:10.1021/ml400501x

Reference yield:

: 865233-37-0
(3S)-3-[4-(4'-trifluoromethyl-biphenyl-3-ylmethoxy)-phenyl]-hex-4-ynoic acid methyl ester

: 916219-96-0
C₂₅H₂₂F₃NO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen; quinoline / ethyl acetate / 8 h / Inert atmosphere

2.1: 2,6-dimethylpyridine; osmium(VIII) oxide / water; tert-butyl alcohol / 0.08 h

2.2: 20 - 30 °C

3.1: potassium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 3 h / -5 - 0 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonia / dichloromethane; propan-1-ol / 8 h / Inert atmosphere

With 2,6-dimethylpyridine; quinoline; sodium chlorite; potassium dihydrogenphosphate; osmium(VIII) oxide; ammonia; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In propan-1-ol; dichloromethane; water; ethyl acetate; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ml400501x

Reference yield:

: C₂₇H₂₅F₃O₃

: 916219-96-0
C₂₅H₂₂F₃NO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-dimethylpyridine; osmium(VIII) oxide / water; tert-butyl alcohol / 0.08 h

1.2: 20 - 30 °C

2.1: potassium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 3 h / -5 - 0 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonia / dichloromethane; propan-1-ol / 8 h / Inert atmosphere

With 2,6-dimethylpyridine; sodium chlorite; potassium dihydrogenphosphate; osmium(VIII) oxide; ammonia; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In propan-1-ol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ml400501x