N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Base Information

Chemical Name:N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide
CAS No.:1362317-64-3
Molecular Formula:C₃₈H₃₇N₇O₆
Molecular Weight:687.755
Hs Code.:

Synonyms:N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

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Chemical Property of N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

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Technology Process of N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

There total 4 articles about N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1362317-68-7
C₁₇H₁₉N₇O₄

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1362317-64-3
N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Guidance literature:: With pyridine; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.104

Reference yield:

: 1362317-63-2
C₂₃H₃₃N₇O₄Si

: 1362317-64-3
N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / dichloromethane / 4 h

2: pyridine / 20 °C / Inert atmosphere

With pyridine; triethylamine tris(hydrogen fluoride); In dichloromethane;
DOI:10.1016/j.bmcl.2011.12.104

Reference yield:

: 168263-86-3
N⁴-benzoylcytosine-1-acetic acid

: 1362317-64-3
N-(1-(2-((2-azidoethyl)(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)amino)-2-oxoethyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; N,N-dimethyl-formamide / 20 °C / Cooling with ice

2: triethylamine tris(hydrogen fluoride) / dichloromethane / 4 h

3: pyridine / 20 °C / Inert atmosphere

With pyridine; triethylamine tris(hydrogen fluoride); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.12.104