1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Base Information

Chemical Name:1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene
CAS No.:194483-69-7
Molecular Formula:C₂₁H₃₅N₇
Molecular Weight:385.556
Hs Code.:

Synonyms:1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Suppliers and Price of 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

There total 2 articles about 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 340722-54-5
1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene

: 194483-69-7
1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Guidance literature:: With trifluoroacetic acid; for 2h;
DOI:10.1002/chem.200305737

Reference yield:

: 1-{[(1,1-dimethylethoxy)carbonyl]aminomethyl}-3,5-bis(aminomethyl)-2,4,6-triethylbenzene dihydro diacetate

: 194483-69-7
1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / 72 h / 100 °C

2: 100 percent / aq. CF₃COOH / 2 h

With trifluoroacetic acid;
DOI:10.1002/chem.200305737

Reference yield: 99.0%

: 40138-16-7
2-formylbenzene boronic acid

: 194483-69-7
1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

: C₂₈H₄₁BN₇O₂^(1-)*H⁽¹⁺⁾

Guidance literature:: 2-formylbenzene boronic acid; 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene; With 3 A molecular sieve; triethylamine; In methanol; at 25 ℃; for 3h;

With sodium tetrahydroborate; 3 A molecular sieve; In methanol; at 25 ℃; for 1h;
DOI:10.1002/(SICI)1521-3773(19991216)38:24<3666::AID-ANIE3666>3.0.CO;2-E