1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene

Base Information

• Chemical Name: 1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene
• CAS No.: 340722-54-5
• Molecular Formula: C₂₆H₄₃N₇O₂
• Molecular Weight: 485.673

Synonyms:1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene

Chemical Property of 1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene

Chemical Property:

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Technology Process of 1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene

There total 1 articles about 1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2-methylthioimidazoline (20112-79-2) + 1-{[(1,1-dimethylethoxy)carbonyl]aminomethyl}-3,5-bis(aminomethyl)-2,4,6-triethylbenzene dihydro diacetate → 1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene (340722-54-5)

Guidance literature:

at 100 ℃; for 72h;

DOI:10.1002/chem.200305737

Reference yield: 100.0%

1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene (340722-54-5) → 1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene (194483-69-7)

Guidance literature:

With trifluoroacetic acid; for 2h;

DOI:10.1002/chem.200305737

Reference yield:

1-[[(1,1-dimethylethoxy)carbonyl]aminomethyl]-3,5-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-2,4,6-triethylbenzene (340722-54-5) → C28H40BN7O2

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / aq. CF₃COOH / 2 h

2: Et₃N; 3 Angstroem molecular sieves / methanol / 3 h / 25 °C

With 3 A molecular sieve; triethylamine; trifluoroacetic acid; In methanol;

DOI:10.1002/chem.200305737

upstream raw materials:

2-methylthioimidazoline

Downstream raw materials:

1,3-bis((4,5-dihydro-1H-imidazol-2-yl)aminomethyl)-5-aminomethyl-2,4,6-triethylbenzene

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