disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

Base Information

Chemical Name:disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate
CAS No.:25845-45-8
Molecular Formula:C₂₄H₁₅ClN₆O₉S₂*2Na
Molecular Weight:676.982
Hs Code.:

Synonyms:disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

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Chemical Property of disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

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Technology Process of disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

There total 4 articles about disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: MG 40-1

: 25845-45-8
disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

Guidance literature:: at 60 ℃; for 0.5h;
DOI:10.1021/jm9003297

Reference yield: 96.0%

: 67-56-1
methanol

: C₂₄H₁₃Cl₂N₆O₇S^(1-)*2Na⁽¹⁺⁾

: 25845-45-8
disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

Guidance literature:: at 60 ℃; for 0.5h;
DOI:10.1021/jm1012193

Reference yield:

: 535-87-5
3.5-diaminobenzoic acid

: 25845-45-8
disodium 1-amino-4-[4-(4-chloro-6-methoxy[1,3,5]triazine-2-ylamino)-3-sulfophenylamino]-9,10-dioxo-9,10-dihydroanthracene-2-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: copper / pH 6 - 7 / Phosphate buffer; Microwave irradiation

2: water; acetone / 0 - 20 °C

3: 0.5 h / 60 °C

With copper; In water; acetone; 1: Ullmann type reaction;
DOI:10.1021/jm1012193