4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile

Base Information

• Chemical Name: 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile
• CAS No.: 269054-88-8
• Molecular Formula: C₂₀H₁₈BrN₅
• Molecular Weight: 408.3

Synonyms:4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile

Chemical Property of 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile

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Technology Process of 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile

There total 4 articles about 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

5-bromo-4-chloro-N-(2,4,6-trimethylphenyl)-2-pyrimidinamine (269055-64-3) + 4-Aminobenzonitrile (873-74-5) → 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile (269054-88-8) + C20H18ClN5

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; diethyl ether; for 96h; Inert atmosphere; Reflux;

Reference yield:

1,4-dioxane (123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6) + 4-[[5-chloro-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile (269054-87-7) + diethyl ether (60-29-7,927820-24-4) + 4-Aminobenzonitrile (873-74-5) → 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile (269054-88-8)

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane;

Reference yield:

1,4-dioxane (123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6) + 5-bromo-4-chloro-N-(2,4,6-trimethylphenyl)-2-pyrimidinamine (269055-64-3) + diethyl ether (60-29-7,927820-24-4) + 4-Aminobenzonitrile (873-74-5) → 4-[[5-bromo-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile (269054-88-8) + 4-[[5-chloro-2-[(2,4,6-trimethylphenyl)amino]-4-pyrimidinyl]amino]benzonitrile (269054-87-7)

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane;

upstream raw materials:

1,4-dioxane

5-bromo-4-chloro-N-(2,4,6-trimethylphenyl)-2-pyrimidinamine

diethyl ether

4-Aminobenzonitrile

Downstream raw materials:

4-[[5-bromo-4-[(2,4,6-trimethylphenyl)amino]-2-pyrimidinyl]amino]benzonitrile

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