endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

Base Information

Chemical Name:endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane
CAS No.:119184-54-2
Molecular Formula:C₂₅H₂₆N₂
Molecular Weight:354.495
Hs Code.:

Synonyms:endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

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Technology Process of endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

There total 2 articles about endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 119184-53-1
endo-6-benzyl-7-<3,3-(trimethylenedioxy)propyl>-4-vinylidene-6-azabicyclo<3.2.1>octane

: 100-63-0
phenylhydrazine

: 119184-54-2
endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

Guidance literature:: With sulfuric acid; In water; for 16h; Heating;
DOI:10.1021/ja00189a036

Reference yield:

: 108634-66-8
(1S,5S)-6-Benzyl-4-vinylidene-6-aza-bicyclo[3.2.1]octan-7-one

: 119184-54-2
endo-6-benzyl-7-(3'-indolylmethyl)-4-vinylidene-6-azabicyclo<3.2.1>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaBH₃CN / 1.) THF, 0 deg C, 30 min; room temp., 18 h, 2.) acetic acid; room temp., 1.5 h

2: 32 percent / H₂SO₄ / H₂O / 16 h / Heating

With sulfuric acid; sodium cyanoborohydride; In water;
DOI:10.1021/ja00189a036