Technology Process of C64H87Br2NO5S2
There total 7 articles about C64H87Br2NO5S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
chloroform;
at 0 - 20 ℃;
for 1.25h;
DOI:10.1021/ma902762z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 3 h / Reflux; Inert atmosphere
2.1: sodium hydride / tetrahydrofuran / 0.08 h / Inert atmosphere; Reflux
2.2: 2 h / Inert atmosphere; Reflux
3.1: sodium hydride / tetrahydrofuran / 1 h / Reflux
4.1: N-Bromosuccinimide / chloroform / 1.25 h / 0 - 20 °C
With
N-Bromosuccinimide; sodium hydride;
In
tetrahydrofuran; chloroform;
1.1: Arbuzov reaction / 2.1: Wittig-Horner reaction / 3.1: Wittig-Horner coupling;
DOI:10.1021/ma902762z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 0.25 h
1.2: 19 h / Reflux
1.3: 1.5 h / 20 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / Reflux
3.1: N-Bromosuccinimide / chloroform / 1.25 h / 0 - 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); N-Bromosuccinimide; sodium hydride; sodium t-butanolate;
In
tetrahydrofuran; chloroform; toluene;
1.1: Buchwald-Hartwig reaction / 1.2: Buchwald-Hartwig reaction / 2.1: Wittig-Horner coupling;
DOI:10.1021/ma902762z