lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Base Information

Chemical Name:lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate
CAS No.:1114761-92-0
Molecular Formula:C₄₃H₃₉N₆O₃*Li
Molecular Weight:694.762
Hs Code.:

Synonyms:lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Suppliers and Price of lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Hazard Codes:

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Technology Process of lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

There total 9 articles about lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144690-33-5
ethyl 4-(2-hydroxypropan-2-yl)-2-propyl-1-({2'-[1-(triphenylmethyl)-1H-1,2,3,4-tetrazol-5-yl]-[1,1'-biphenyl]-4-yl}methyl)-1H-imidazole-5-carboxylate

: 1114761-92-0
lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Guidance literature:: With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

Reference yield:

: 144690-33-5
ethyl 4-(2-hydroxypropan-2-yl)-2-propyl-1-({2'-[1-(triphenylmethyl)-1H-1,2,3,4-tetrazol-5-yl]-[1,1'-biphenyl]-4-yl}methyl)-1H-imidazole-5-carboxylate

: 124-38-9,18923-20-1
carbon dioxide

: 1114761-92-0
lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Guidance literature:: With lithium hydroxide monohydrate; sodium chloride; In 1,4-dioxane; water; ethyl acetate;

Reference yield:

: 155983-56-5
5-<2-(4'-formylbiphenylyl)>-2-(triphenylmethyl)-2H-tetrazole

: 1114761-92-0
lithium 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 5 - 20 °C

1.2: 0.25 h / 0 °C

2.1: phosphorus tribromide / dichloromethane / 1 h / 10 - 20 °C

3.1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 100 °C

4.1: lithium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium hydroxide; lithium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;