1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

Base Information

Chemical Name:1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester
CAS No.:1024613-07-7
Molecular Formula:C₂₅H₂₆O₆
Molecular Weight:422.478
Hs Code.:

Synonyms:1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

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Chemical Property of 1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

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Technology Process of 1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

There total 3 articles about 1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 100-39-0
benzyl bromide

: 103008-86-2
4,5-Dihydroxy-3,5-cyclopentadien-1,3-dicarbonsaeure-diethylester

: 1024613-07-7
1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; for 16h; Heating;
DOI:10.1016/j.tetasy.2008.01.028

Reference yield: 47.0%

: C₁₁H₁₂O₆^(2-)*2K⁽¹⁺⁾

: 100-39-0
benzyl bromide

: 1024613-07-7
1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.5b01963

Reference yield:

: 818-38-2
Diethyl glutarate

: 100-39-0
benzyl bromide

: 95-92-1
oxalic acid diethyl ester

: 1024613-07-7
1-benzyl-4-benzyloxy-5-oxo-cyclopent-3-ene-1,3-dicarboxylic acid diethyl ester

Guidance literature:: Diethyl glutarate; oxalic acid diethyl ester; With potassium tert-butylate; In tetrahydrofuran; for 0.5h; Heating;

benzyl bromide; In N,N-dimethyl-formamide; at 120 ℃; for 2h; Further stages.;
DOI:10.1016/j.tetasy.2008.01.028